Sintesis dan Karakterisasi Feâ‚‚TiOâ‚… dari Besi Oksida dan Titanium Dioksida dengan Metode Planetary Ball-Mill: Synthesis and Characterization of Feâ‚‚TiOâ‚… from Iron Oxide and Titanium Dioxide Using the Planetary Ball-Mill Method

Laode Kadir; M. H Azis; S.  Musiam; V. A.  Fabiani; Karnelasatri; D.  Permana; T Azis; Syahrir

doi:10.22487/kovalen.2022.v8.i3.15644

Authors

Laode Kadir a:1:{s:5:"en_US";s:21:"Universitas Halu Oleo";}
M. H Azis Jurusan Kimia, Universitas Mataram
S. Musiam Jurusan Kimia, Sekolah Tinggi Ilmu Kesehatan ISFI Banjarmasin
V. A. Fabiani Jurusan Kimia, Universitas Bangka Belitung
Karnelasatri Jurusan Farmasi, Universitas Pelita Harapan
D. Permana Jurusan Kimia, Universitas Sembilan Belas November Kolaka
T Azis Jurusan Kimia, Fakultas Matematika dan Ilmu Pengetahuan Alam,Universitas Halu Oleo
Syahrir Jurusan Kimia, Fakultas Matematika dan Ilmu Pengetahuan Alam,Universitas Halu Oleo

DOI:

https://doi.org/10.22487/kovalen.2022.v8.i3.15644

Abstract

The method of solid hydrogen storage through integration in metal hydride compounds is a new, promising method. This research has succeeded in synthesizing and characterizing the metal hydride alloy Fe-Ti system through a planetary ball-mill process. Based on the XRF analysis, it was found that the composition of Fe oxide content reached 56.22% while Ti oxide reached 43.78%. The FTIR study showed absorption at wavenumbers of 900 cm^-1 and 500 cm^-1. Both are typical absorptions for Ti-O and Fe-O groups, suggesting that the synthesized sample was successful. It can be seen from the XRD data that some of the diffractogram peaks of the resulting Fe-Ti compound match the peaks of the Fe₂TiO₅ and TiO₂ compounds obtained from the Powder Diffraction File (PDF) database number 00-003-0374. After the refinement was performed, information was obtained that the synthesis of Fe-Ti alloy material using the planetary ball mill technique produced Fe₂TiO₅.